Passivation Time & Temperature Calculator | ASTM A967 Compliance | CXP Solutions
⏱️ ASTM A967 Compliant

Passivation Time & Temperature Calculator

Calculate required contact time and temperature for stainless steel passivation. Supports citric acid and nitric acid methods per ASTM A967, AMS 2700, and pharmaceutical requirements.

ASTM
A967 Compliant
AMS
2700 Standards
cGMP
Pharma Ready
°F
15 min minimum

Calculate Passivation Parameters

Enter your specifications to determine required contact time, temperature range, and complete procedure

⚗️ Passivation Parameters

Citric Acid (Chelant Method)
Nitric Acid (Oxidizing Method)
Citric Acid + Additives
Austenitic (300 Series)
304/304L
316/316L
321
317L
Duplex & Specialty
2205 Duplex
Hastelloy C-276
Inconel 625
New/Clean (No contamination)
Machined (Light oil/cutting fluid)
Post-Weld (Heat tint, scale)
Heavily Contaminated/Rouge
ASTM A967 (General)
AMS 2700 (Aerospace)
Pharmaceutical (cGMP)
Semiconductor (UHP)

Disclaimer: This calculator is provided for informational purposes only. Always verify parameters with applicable specifications and perform validation testing.

⏱️

Ready to Calculate

Enter your passivation parameters on the left and click "Calculate" to see required contact time, temperature range, and complete specifications.

✅ Passivation Specifications
-
Minimum Contact Time
-
Temperature Range
-
Total Cycle Time
Temperature Zone
60°F (Cold) 90°F 120°F (Optimal) 150°F 180°F (Hot)
Passivation Cycle Timeline
🧹
Pre-Clean
5 min
💧
Rinse
3 min
⚗️
Passivate
15 min
🚿
Final Rinse
5 min
Test
-
📋 Procedure: Results will appear here after calculation.
Temperature + Time = Complete Passivation

Every 10°F increase roughly doubles the reaction rate. Optimize your parameters for faster cycles without compromising quality.

Citric vs. Nitric Acid Passivation

Compare the two primary passivation methods to choose the best approach for your application

🍋
Citric Acid
Chelant Method
4-10%
Concentration
70-160°F
Temperature
10-30 min
Contact Time
Low
Hazard Level
  • Environmentally friendly & biodegradable
  • No NOx fumes or hazardous disposal
  • Excellent for pharmaceutical applications
  • Works well on all 300-series alloys
  • Better rouge removal capability
  • Lower equipment corrosion risk
VS
⚗️
Nitric Acid
Oxidizing Method
20-25%
Concentration
70-130°F
Temperature
20-30 min
Contact Time
High
Hazard Level
  • Traditional industry standard method
  • Strongly oxidizing for thick oxide layer
  • Required by some legacy specifications
  • Effective scale and smut removal
  • Lower chemical cost per gallon
  • Faster brightening effect

Alloy Passivation Guide

Passivation difficulty and recommended parameters by alloy type

304/304L
Austenitic Stainless
Easy
Standard citric or nitric. Most forgiving alloy. 15-20 min at 120°F typical.
316/316L
Austenitic Stainless
Easy
Higher Mo content aids passivation. Citric preferred for pharma. 15-20 min at 120°F.
321
Stabilized Austenitic
Medium
Ti-stabilized. May need slightly longer time. 20-25 min at 130°F recommended.
317L
High-Mo Austenitic
Easy
Extra Mo makes it very easy to passivate. 15 min at 120°F often sufficient.
2205
Duplex Stainless
Medium
Dual-phase structure. Citric preferred. 20-30 min at 130-140°F for best results.
Hastelloy C-276
Ni-Mo-Cr Alloy
Difficult
High Ni content. Citric only (nitric can attack). 30-45 min at 140°F.
Inconel 625
Ni-Cr-Mo Alloy
Difficult
Very high Ni. Requires citric acid only. 30-45 min at 130-140°F minimum.
AL-6XN
Super Austenitic
Medium
High Mo super alloy. Citric preferred. 20-30 min at 130°F for complete passivation.

ASTM A967 Standard Parameters

Minimum requirements by method per ASTM A967 specification

Method Chemical Concentration Temperature Time Best For
Citric 3 Citric Acid 4-10% w/w 70-160°F 4-30 min All 300 series, general use
Citric 7 Citric + Additives 4-10% w/w 120-140°F 10-30 min Enhanced cleaning, rouge removal
Nitric 5 Nitric Acid 20-25% 70-130°F 20-30 min 304, 304L, 321, free-machining
Nitric 6 Nitric Acid 20-25% 120-130°F 20-30 min 316, 316L, 317L, high-Mo alloys
Nitric 7 Nitric + Dichromate 20% + 2-3% 120-160°F 20-30 min 300 + 400 series, aggressive
Chelant Proprietary Per mfg 100-140°F 15-60 min All grades, specialty applications
📘 Note: These are minimum ASTM A967 requirements. Actual parameters may vary based on contamination level, part geometry, customer specifications, and validation testing. Always verify final parameters through appropriate acceptance testing per ASTM A380.

Frequently Asked Questions

How does temperature affect passivation time?

Temperature has an exponential effect on reaction rate. Every 10°F increase roughly doubles the rate, allowing shorter contact times. At 140°F, citric acid may need only 10-15 minutes vs. 25-30 minutes at 70°F. However, temperatures above 160°F can cause etching or decomposition.

What happens if contact time is too short?

Insufficient time results in incomplete chromium oxide formation, leaving free iron that will corrode. This leads to copper sulfate test failures, early corrosion, and potential product contamination. Always meet or exceed minimum times.

Why does 316L need different parameters than 304?

316L has higher nickel and molybdenum content, changing passivation kinetics. It typically requires higher temperatures (120-130°F minimum) for nitric acid. Citric acid works well at moderate temperatures. The higher alloy content makes 316L more forgiving.

Can I use higher concentration to reduce time?

Yes, within limits. Increasing citric from 6% to 10% can reduce time by 30-40%. However, above 10% provides no additional benefit. For nitric, above 25% causes excessive etching. It's often better to increase temperature slightly instead.

Do contaminated parts need longer time?

Yes. Parts with heavy rouge, weld scale, or iron contamination may need 2-3× normal time, or pre-cleaning before passivation. Some cases require an initial derouging step at 10-15% citric for 30-60 minutes before final passivation.

Which method is better for pharmaceutical applications?

Citric acid is strongly preferred for pharmaceutical and biotech. It's safer to handle, environmentally friendly, produces no hazardous fumes, and is easier to validate. Most pharma facilities have moved away from nitric acid entirely.

Need Professional Passivation Services?

CXP Solutions provides ASTM A967 and AMS 2700 compliant passivation with validated procedures, complete documentation, and nationwide service. We handle all aspects from pre-cleaning through final testing.

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